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4.2.2.2.1 Characteristic frequencies IR spectroscopy is often used for the first approximate characterization of a new compound, since it is a fast and simple method. Over the past few years, Raman spectroscopy has also gained significance as new techniques (e.g., FT methods) were developed. It is especially in inorganic chemistry that Raman spectroscopy has a considerable advantage over IR methods, since sensitive samples can be measured in closed glass tubes. In order to interpret vibrational spectra, one often starts with the simple concept that typical frequencies can be related to certain pairs of atoms. Absorptions in certain frequency ranges should provide information about particular groups of atoms in the unknown species. Typical ranges of frequencies of stretching vibrations of organic compounds as well as of bending vibrations, e.g., p(CH2); 7(CH2), w(CH2) are listed in Section 4.1 (Table 4.1-1, Figure 4.1-1) of this book. On the other hand, it is more difficult to discuss vibrational spectra of inorganic compounds, since, due to the size of the periodic table, a wide variety of heterogeneous bonding occurs. Therefore, two books containing only tables of stretching vibrations have been published (Weidlein et al., 1981 and 1986). The frequencies of diatomic species provide a starting point for the assignment of vibrations in larger molecules. However, the situation in diatomic molecules is fundamentally different from that in larger molecules, as in the latter case coupling has to be taken into account (see also Sec. 2.5). Without critical consideration of such influences,

A centralized location, either physical or virtual, for the storage, management, and control of the data and information for a particular body organization or business. Data change log a log that stores updates to the primary as the associated snapshot volume was created. It is used for mirror fast resynchronization. The process of converting encrypted data back into its original form, so it can be understood. Dynamic host con guration protocol TCP/ IP protocol that automatically assigns temporary IP addresses to hosts when they connect to the network. A backup that copies the les that have changed as the last successful backup of any kind. All les are backed up if no prior backup has been done. The act or process of recovering data from backups after a disk crash or other catastrophe. An automated process for using disk as a cache during the backup process that will move the backed up data from the disk to a secondary location. The process of converting data into a form, called a ciphertext, that cannot be easily understood by unauthorized people. To remove, erase, or completely delete data or references to the data. Most common usage of this is the removal of legal records when requested by the court. The ability to resync a mirror based on a log of the changes made while the mirror is split. A variable portion of a le as determined by the single instance store application. A set of related programs which can be located at a network gateway server that protects the resources of a private network from users to other networks.

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Other properties can be changed simply by setting them to something else and calling the Put() method, which writes them back. Some can only be changed by calling special purpose methods. For example, in the preceding examples, you can see that the volume name is blank. You can set the volume name, save it using Put(), and verify it has been saved with Get().

Figure 2.2-1 Observation of'the excitation of a vibrational state in the eleclronic ground stale SO, by a, infrared absorplion; b, Raman scattering; c , inelastic neutron scattering; d, fluorescence.

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When you declare a variable, you use the AS clause to assign a data type to the variable. Data types for variables are similar to data types in a database table definition.

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