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Thus, the main impurities are water, HCOOH and (CH3)2NH Small amounts of HCN, formed by photolysis, and CO, formed by thermal decomposition, are also present In the purification of a commercial product, it is kept with molecular sieves (4A or 5A) for 1 4 days to dehydrate Then it is shaken with BaO for 1 2 days and the supernatant is distilled twice at 20 mmHg under nitrogen All these operations must be carried out in the absence of light The distillate should be stored under nitrogen gas and used as soon as possible DMF has toxic effects, particularly on the liver and kidney and care should be taken in its handling Dimethyl sulfoxide (DMSO) [14]: Commercial products contain water and small amounts of dimethyl sulfide and dimethyl sulfone as impurities. rdlc pdf 417 PDF417 Barcode Creating Library for RDLC Reports | Generate ...
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